Invitation to the 4th InterLaboratory Comparison of NMR techniques

 

Experiment Time

30h

Experiment Time

The expected machine time needed for the experiment is 30h

Samples Tube

8

Samples Tube

Wil be provided 8 sealed sample tube for NMR Testing

Reference Tube

1

Reference Tube

A sealed sample tube for NMR reference will be provided

Participation Cost

FREE

Participation Cost

All the shipment and sample production cost will be covered by Innovative Solutions

Founded by project IPERDURUM – FILIERA FRUMENTO DURO: INNOVAZIONE VARIETALE,QUALITA’ E TRACCIABILITA’ DELLE PRODUZIONI PUGLIESI

ILC4 Milestones

22/07/15 to 22/10/05

Applications [COMPLETED]

22/10/06 to 22/11/30

Sample preparation and Shipment

22/12/01 to 23/01/31

Results collection

23/01/16 to 23/02/28

Data elaboration and report publication

What's the Interlaboratory Comparison

With the support of the project IPERDURUM, Innovative Solution and SAMER are launching the 4th Interlaboratory Comparison for NMR spectrometer.

You are invited to apply with your spectrometer to ensure a better understanding of NMR techniques and futher improve the technique.

Innovative Solutions organizes NMR Interlaboratory Comparisons (NMR-ILCs) according to ISO/IEC 17043:2010 and reference normative therein. NMR-ILCs provide objective standards for individual laboratories, allow them to compare analytical results from different laboratories and represent a way to check the quality and the accuracy of the analytical job. Validation by ILCs is the starting point for official recognition of the analytical methods.

 

ILC Documentation

Experiment Detail

NMR tubes provided to participants: 11.

    • Aqueous extracts of wheat samples will be contained in 5 NMR tubes.
    • Aqueous extracts of pasta samples will be contained in 4 NMR tubes.

The tubes will contain buffered aqueous extracts of wheat (or pasta), sodium azide as biocide and 3-(trimethylsilyl)-2,2,3,3-tetradeuteropropanoic acid sodium salt in D2O, as internal reference.

External Standard: DMSO2. 1 NMR tube

Deuterated methanol will be contained in 1 NMR tube.

ILC scientific production

Published 2020

https://dx.doi.org/10.1016/j.talanta.2020.120855

Published 2020

https://dx.doi.org/10.1007/s12161-019-01664-8

Published 2015

https://dx.doi.org/10.1021/acs.analchem.5b00919

Scientific Committee

Vito Gallo, Polytechnic University of Bari, Innovative Solutions S.r.l., Italy
Biagia Musio, Polytechnic University of Bari, Innovative Solutions S.r.l., Italy
Rosa Ragone, Polytechnic University of Bari, Italy
Marica Antonicelli, Polytechnic University of Bari, Italy
Stefano Todisco, Polytechnic University of Bari, Italy

Maurizio Triggiani, Innovative Solutions S.r.l., Italy
Trisolini Maria, Innovative Solutions S.r.l., Italy
Piero Mastrorilli, Polytechnic University of Bari, Innovative SolutionsS.r.l., Italy
Mario Latronico, Polytechnic University of Bari, Innovative Solutions S.r.l., Italy

Application

The application phase has ended

Satisfying the need for varietal innovation for durum wheat crops, an indispensable tool for offering high value-added productions, ensuring product healthiness and preventing the risk of the development of mycotoxins.

“Fondo europeoagricolo per lo sviluppo rurale: l’Europa investe nelle zone rurali” PSR 2014-2020. MISURA 16.2 Focus Area 2a) – Progetto: FILIERA FRUMENTO DURO: INNOVAZIONE VARIETALE,QUALITA’ E TRACCIABILITA’ DELLE PRODUZIONI PUGLIESI – Acronimo IPERDURUM –

www.psr.regione.puglia.it

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Melbourne, Australia
(Sat - Thursday)
(10am - 05 pm)