The expected machine time needed for the experiment is 30h
Samples Tube
8
Samples Tube
Wil be provided 8 sealed sample tube for NMR Testing
Refernece Tube
4
Refernece Tube
Wil be provided 4 sealed sample tube for NMR reference
Participation Cost
FREE
Participation Cost
All the shipment and sample production cost will be covered by Innovative Solutions
Max Participants
50
Max Participants
We'll limit the number of laboratory to ensure timely execution of ILC
Founded by project IPERDURUM – FILIERA FRUMENTO DURO: INNOVAZIONE VARIETALE,QUALITA’ E TRACCIABILITA’ DELLE PRODUZIONI PUGLIESI
What's the Interlaboratory Comparison
With the support of the project IPERDURUM, Innovative Solution and SAMER are launching the 4th Interlaboratory Comparison for NMR spectrometer.
You are invited to apply with your spectrometer to ensure a better understanding of NMR techniques and futher improve the technique.
Innovative Solutions organizes NMR Interlaboratory Comparisons (NMR-ILCs) according to ISO/IEC 17043:2010 and reference normative therein. NMR-ILCs provide objective standards for individual laboratories, allow them to compare analytical results from different laboratories and represent a way to check the quality and the accuracy of the analytical job. Validation by ILCs is the starting point for official recognition of the analytical methods.
Aqueous extracts of wheat samples will be contained in 5 NMR tubes.
Aqueous extracts of pasta samples will be contained in 4 NMR tubes.
The tubes will contain buffered aqueous extracts of wheat (or pasta), sodium azide as biocide and 3-(trimethylsilyl)-2,2,3,3-tetradeuteropropanoic acid sodium salt in D2O, as internal reference.
External Standard: DMSO2. 1 NMR tube
Deuterated methanol will be contained in 1 NMR tube.
ILC scientific production
Published 2020
https://dx.doi.org/10.1016/j.talanta.2020.120855
Published 2020
https://dx.doi.org/10.1007/s12161-019-01664-8
Published 2015
https://dx.doi.org/10.1021/acs.analchem.5b00919
ILC4 Milestones
22/07/15 to 22/10/05
Applications
22/10/06 to 22/11/30
Sample preparation and Shipment
22/12/01 to 23/01/15
Results collection
23/01/16 to 23/02/28
Data elaboration and report publication
Scientific Committee
Vito Gallo, Polytechnic University of Bari, Innovative Solutions S.r.l., Italy Biagia Musio, Polytechnic University of Bari, Innovative Solutions S.r.l., Italy Rosa Ragone, Polytechnic University of Bari, Italy Marica Antonicelli, Polytechnic University of Bari, Italy Stefano Todisco, Polytechnic University of Bari, Italy
Maurizio Triggiani, Innovative Solutions S.r.l., Italy Trisolini Maria, Innovative Solutions S.r.l., Italy Piero Mastrorilli, Polytechnic University of Bari, Innovative SolutionsS.r.l., Italy Mario Latronico, Polytechnic University of Bari, Innovative Solutions S.r.l., Italy
Application
Satisfying the need for varietal innovation for durum wheat crops, an indispensable tool for offering high value-added productions, ensuring product healthiness and preventing the risk of the development of mycotoxins.
“Fondo europeoagricolo per lo sviluppo rurale: l’Europa investe nelle zone rurali” PSR 2014-2020. MISURA 16.2 Focus Area 2a) – Progetto: FILIERA FRUMENTO DURO: INNOVAZIONE VARIETALE,QUALITA’ E TRACCIABILITA’ DELLE PRODUZIONI PUGLIESI – Acronimo IPERDURUM –
www.psr.regione.puglia.it
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