Invitation to the 4th InterLaboratory Comparison of NMR techniques

Admissions closes in

Experiment Time

30h

Experiment Time

The expected machine time needed for the experiment is 30h

Samples Tube

Wil be provided 8 sealed sample tube for NMR Testing

Refernece Tube

Wil be provided 4 sealed sample tube for NMR reference

Participation Cost

FREE

Participation Cost

All the shipment and sample production cost will be covered by Innovative Solutions

Max Participants

We'll limit the number of laboratory to ensure timely execution of ILC

With the support of the project IPERDURUM, Innovative Solution and SAMER are launching the 4th Interlaboratory Comparison for NMR spectrometer.

You are invited to apply with your spectrometer to ensure a better understanding of NMR techniques and futher improve the technique.

Innovative Solutions organizes NMR Interlaboratory Comparisons (NMR-ILCs) according to ISO/IEC 17043:2010 and reference normative therein. NMR-ILCs provide objective standards for individual laboratories, allow them to compare analytical results from different laboratories and represent a way to check the quality and the accuracy of the analytical job. Validation by ILCs is the starting point for official recognition of the analytical methods.

Discover the previous ILC

NMR tubes provided to participants: 11.

- Aqueous extracts of wheat samples will be contained in 5 NMR tubes.
- Aqueous extracts of pasta samples will be contained in 4 NMR tubes.

The tubes will contain buffered aqueous extracts of wheat (or pasta), sodium azide as biocide and 3-(trimethylsilyl)-2,2,3,3-tetradeuteropropanoic acid sodium salt in D₂O, as internal reference.

External Standard: DMSO_2.1 NMR tube

Deuterated methanol will be contained in 1 NMR tube.

Published 2020

Published 2015

22/07/15 to 22/10/05

Applications

22/10/06 to 22/11/30

Sample preparation and Shipment

22/12/01 to 23/01/15

Results collection

23/01/16 to 23/02/28

Data elaboration and report publication

Vito Gallo, Polytechnic University of Bari, Innovative Solutions S.r.l., Italy
Biagia Musio, Polytechnic University of Bari, Innovative Solutions S.r.l., Italy
Rosa Ragone, Polytechnic University of Bari, Italy
Marica Antonicelli, Polytechnic University of Bari, Italy
Stefano Todisco, Polytechnic University of Bari, Italy

Maurizio Triggiani, Innovative Solutions S.r.l., Italy
Trisolini Maria, Innovative Solutions S.r.l., Italy
Piero Mastrorilli, Polytechnic University of Bari, Innovative SolutionsS.r.l., Italy
Mario Latronico, Polytechnic University of Bari, Innovative Solutions S.r.l., Italy

Application

Invitation to the 4th InterLaboratory Comparison

Laboratory Name

Principal Investigator

Email of the PI

Spectrometer Information

NMR Spectrometer Model

Probehead information

BBI, BBO, TBI, cryo-probe, cold probe, etc.

NMR Spectrometer Manufacturer

Magnetic Field

Larmor frequency for ¹H

NMR Spectrometer Production year

Affiliation Information

Affiliation of the PI

Address

Country

City

State

ZIP Code

VAT Number

Shipment Information

Send sample to

Contact Person

Affiliation of the Contact Person

if differnt from Affiliation of the PI

Address

Used for the samples shipment if different from Affiliation address

Country

City

State

ZIP Code

Notes

Contact Person Phone Number

Contact Person email

By submitting this application, I ask for activation/confirmation of the online NMR Spectrometer Profile to be used for participation in NMR Interlaboratory Comparisons organized by Innovative Solutions S.r.l. (IS-NMR-ILC).
By submitting this application, I ask for participation in the IS-NMR-ILC 001_2022 by using the NMR spectrometer indicated above.
I am aware that:
1. activation of the NMR Spectrometer Profile is free of charge;
2. participation in IS-NMR-ILCs requires compliance with the “IS-NMR-ILC Scheme” and with the “Call for participation” of the comparison.
Moreover, I declare that PRINCIPAL INVESTIGATOR or the Affiliated Institution will never demand economic contribution for any reason related to its registration in the Interlaboratory Comparison platform of Innovative Solutions S.r.l.
By submitting this application, I authorize Innovative Solutions S.r.l. to share NMR data, either entirely or partly, with third parties provided that the identity of my laboratory remains undisclosed.

by submitting this form I consent to the above prescriptions, number 1, 2, 3, 3.1, 3.2, 4, 5

by submitting this form I consent Innovative Solutions to use my data to be used for the ILC4 organization according to GDPR

Read mora about our privacy policy and GDPR

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