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Invitation to the 4th InterLaboratory Comparison of NMR techniques

Admissions closes in

Experiment Time

30h

Experiment Time

The expected machine time needed for the experiment is 30h

Samples Tube

8

Samples Tube

Wil be provided 8 sealed sample tube for NMR Testing

Refernece Tube

4

Refernece Tube

Wil be provided 4 sealed sample tube for NMR reference

Participation Cost

FREE

Participation Cost

All the shipment and sample production cost will be covered by Innovative Solutions

Max Participants

50

Max Participants

We'll limit the number of laboratory to ensure timely execution of ILC

Founded by project IPERDURUM – FILIERA FRUMENTO DURO: INNOVAZIONE VARIETALE,QUALITA’ E TRACCIABILITA’ DELLE PRODUZIONI PUGLIESI

What's the Interlaboratory Comparison

With the support of the project IPERDURUM, Innovative Solution and SAMER are launching the 4th Interlaboratory Comparison for NMR spectrometer.

You are invited to apply with your spectrometer to ensure a better understanding of NMR techniques and futher improve the technique.

Innovative Solutions organizes NMR Interlaboratory Comparisons (NMR-ILCs) according to ISO/IEC 17043:2010 and reference normative therein. NMR-ILCs provide objective standards for individual laboratories, allow them to compare analytical results from different laboratories and represent a way to check the quality and the accuracy of the analytical job. Validation by ILCs is the starting point for official recognition of the analytical methods.

 

ILC Documentation

Experiment Detail

NMR tubes provided to participants: 11.

    • Aqueous extracts of wheat samples will be contained in 5 NMR tubes.
    • Aqueous extracts of pasta samples will be contained in 4 NMR tubes.

The tubes will contain buffered aqueous extracts of wheat (or pasta), sodium azide as biocide and 3-(trimethylsilyl)-2,2,3,3-tetradeuteropropanoic acid sodium salt in D2O, as internal reference.

External Standard: DMSO2. 1 NMR tube

Deuterated methanol will be contained in 1 NMR tube.

ILC scientific production

Published 2020

https://dx.doi.org/10.1016/j.talanta.2020.120855

Published 2020

https://dx.doi.org/10.1007/s12161-019-01664-8

Published 2015

https://dx.doi.org/10.1021/acs.analchem.5b00919

ILC4 Milestones

22/07/15 to 22/10/05

Applications

22/10/06 to 22/11/30

Sample preparation and Shipment

22/12/01 to 23/01/15

Results collection

23/01/16 to 23/02/28

Data elaboration and report publication

Scientific Committee

Vito Gallo, Polytechnic University of Bari, Innovative Solutions S.r.l., Italy
Biagia Musio, Polytechnic University of Bari, Innovative Solutions S.r.l., Italy
Rosa Ragone, Polytechnic University of Bari, Italy
Marica Antonicelli, Polytechnic University of Bari, Italy
Stefano Todisco, Polytechnic University of Bari, Italy

Maurizio Triggiani, Innovative Solutions S.r.l., Italy
Trisolini Maria, Innovative Solutions S.r.l., Italy
Piero Mastrorilli, Polytechnic University of Bari, Innovative SolutionsS.r.l., Italy
Mario Latronico, Polytechnic University of Bari, Innovative Solutions S.r.l., Italy

Application

Invitation to the 4th InterLaboratory Comparison

Spectrometer Information

BBI, BBO, TBI, cryo-probe, cold probe, etc.
Larmor frequency for 1H

Affiliation Information


Shipment Information

Contact Person
if differnt from Affiliation of the PI
Used for the samples shipment if different from Affiliation address
  1. By submitting this application, I ask for activation/confirmation of the online NMR Spectrometer Profile to be used for participation in NMR Interlaboratory Comparisons organized by Innovative Solutions S.r.l. (IS-NMR-ILC).
  2. By submitting this application, I ask for participation in the IS-NMR-ILC 001_2022 by using the NMR spectrometer indicated above.
  3. I am aware that:
    1. activation of the NMR Spectrometer Profile is free of charge;
    2. participation in IS-NMR-ILCs requires compliance with the “IS-NMR-ILC Scheme” and with the “Call for participation” of the comparison.
  4. Moreover, I declare that PRINCIPAL INVESTIGATOR or the Affiliated Institution will never demand economic contribution for any reason related to its registration in the Interlaboratory Comparison platform of Innovative Solutions S.r.l.
  5. By submitting this application, I authorize Innovative Solutions S.r.l. to share NMR data, either entirely or partly, with third parties provided that the identity of my laboratory remains undisclosed.

Satisfying the need for varietal innovation for durum wheat crops, an indispensable tool for offering high value-added productions, ensuring product healthiness and preventing the risk of the development of mycotoxins.

“Fondo europeoagricolo per lo sviluppo rurale: l’Europa investe nelle zone rurali” PSR 2014-2020. MISURA 16.2 Focus Area 2a) – Progetto: FILIERA FRUMENTO DURO: INNOVAZIONE VARIETALE,QUALITA’ E TRACCIABILITA’ DELLE PRODUZIONI PUGLIESI – Acronimo IPERDURUM –

www.psr.regione.puglia.it

At vero eos et accusamus et iusto odio digni goikussimos ducimus qui to bonfo blanditiis praese. Ntium voluum deleniti atque.

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